Analytical Excellence Supporting Environmental Compliance
The EPD Laboratory conducts chemical and microbiological tests to ensure compliance with state and federal environmental regulations. We are an 80-person, multi-disciplinary, integrated laboratory capable of analyzing air, water, soil and biota for a large number of constituents. Working with EPD's regulatory and enforcement staff, the EPD lab helps to ensure Georgia's environment is safe and healthy.
The lab consistently produces analytical results in a high-throughput, high-quality environment:
- In 1993, the lab analyzed 82,000 samples for 150,000 tests and 447,000 analytes
- In 2016, the lab analyzed 120,000 samples for 219,000 tests and 800,000 analytes
- In 2016, the lab passed all audits with a 100% acceptance rate
At the EPD Laboratory, versatility is the key. We have the trained scientists and technicians necessary to perform tasks using a large and diverse group of instrumentation, including:
- Automated Analytic Profile Index (for identification of bacteria)
- AutoAnalyzers (for inorganic analytes)
- Gas Chromatographs (EC, ELCD, FID, MS, NPD)
- Inductively Coupled Argon Plasma Spectrometers (Optical and Mass Spec)
- Ion Chromatographs
- Liquid Chromatographs (Fluorescence, UV/VIS)
Analytical Capability by Matrix and Analysis
Matrix Analysis |
Method |
---|---|
Air |
|
Aldehydes and Ketones |
TO-11 |
Lead From Total Suspended Particulate |
40CFR50, Appendix G |
Particulate Matter-10 |
40CFR50, Appendix J |
Partisol PM-10 |
40CFR50, Appendix J |
Polyaromatic Hydrocarbons |
TO-13 |
Total Suspended Particulates |
40CFR50, Appendix B |
Volatiles |
PAMS |
Volatiles |
TO-154 |
Aqueous Waste |
|
ICP Metals |
6010B |
ICPMS Metals |
6020 |
Mercury |
7470A |
Drinking Water |
|
Carbamate Pesticides |
531.1 |
Chloride |
300.0 |
Chlorinated Pesticides & PCBs |
508.1 |
Chlorinated Acid Herbicides |
515.1 |
Coliforms bacteria |
MMO-MUG (Coliert) |
Diquat |
549.1 |
EDB & DBCP |
504 |
Endothall |
548.1 |
Glyphosate |
547 |
NO3/NO2(Nitrate/Nitrite) |
353.2 |
Nitrogen & Phosphorus Pesticides |
507.1 |
Phthalate & Adipate Esters |
506 |
Polynuclear Aromatics (PNAs) |
550.1 |
Sulfate |
300.0, 375.1 |
TOC (Total Organic Carbon) |
SM5310-D |
Trihalomethanes |
551 |
Volatiles |
524.1 |
Semi-Volatiles |
-525.2 |
Sediment/Soil/Solids |
|
BTEX (Benzene,Toluene,Xylene) |
8021 |
Chlorinated Acid Herbicides |
8150A |
Chlorinated Pesticides & PCBs |
8081 |
Ethylene Glycol |
8015 Mod |
Formaldehyde |
8315 |
ICP Metals |
6010B |
ICPMS Metals |
6020 |
Mercury |
7471A |
Organophosphate Pesticides |
8141A |
Percent Solids & % Volatile Solids |
3540 |
Petroleum Characterization |
8015 Mod |
Semi-Volatile Appendix IX |
8270C |
Semi-Volatiles |
8270C |
TPH Diesel Range |
8015B |
TPH Gasoline Range |
8015B |
Volatile Appendix IX |
8260B |
Volatiles |
5035C/8260B |
Toxicity Characterization Leachate Procedure |
|
ICP Metals |
1311 |
Semi-Volatiles |
1311 |
Volatiles |
1311 |
Waste |
|
Chlorinated Acid Herbicides |
8150 |
Chlorinated Pesticides & PCBs |
8081/8082 |
Cyanide |
9010A |
Formaldehyde |
8315 |
Organophosphate Pesticides |
8141A |
Petroleum Characterization |
8015 |
Semi-Volatile Appendix IX |
8270C |
Semi-Volatiles |
8270C |
Volatile Appendix IX |
8260B |
Volatiles |
8260B |
Water |
|
AA Furnace Metals |
200.9 |
AA Flame Metals |
------- |
Acrolein & Acrylonitrile |
8260B |
Alkalinity |
310.1 |
Analytic Profile Index |
API |
(gram negative bacteria identification) |
|
BOD(Biochemical Oxygen Demand) |
405.1 |
BTEX (Benzene,Toluene,Xylene) |
8020 |
Chloride |
300.0 |
Chlorinated Pesticides & PCBs |
8081 |
Chlorinated Acid Herbicides |
8150A |
COD(Chemical Oxygen Demand) |
410.4 |
Coliforms |
MPN |
Color (all types) |
110.2 |
Cyanide |
SM4500-CN-E |
Cyanide-Amenable |
SM4500-CN-G |
Ethylene Glycol |
8015 Mod |
Fluoride |
SM4500-F-E |
Formaldehyde |
8315 |
Hardness |
130.2 |
Heterotrophic Plate Count |
Std Methods |
ICP Metals |
200.7 |
ICPMS Metals |
200.8 |
MBAS (Surfactant) |
425.1 |
Mercury |
245.2 |
NH3 (Ammonia) |
350.1 |
NO3/NO2(Nitrate/Nitrite) |
353.2 |
Oil & Grease (HEM) |
1664 |
Organophosphate Pesticides |
8141A |
Petroleum Characterization |
8015 Mod |
pH |
150.1 |
Semi-Volatile Appendix IX |
8270C |
Semi-Volatiles |
8270C |
Specific Conductivity |
2510B |
Sulfate |
300.0, 375.1 |
Sulfide |
376.2 |
Tannin & Lignon |
5550 |
TKN (Total Kjeldahl Nitrogen) |
351.1 |
TOC (Total Organic Carbon) |
415.1 |
Total Phenol |
420.2 |
Total & Suspended Solids |
160.3/160.2 |
Total or Ortho Phosphate |
365.1 |
TPH Gasoline Range |
8015B |
TPH Diesel Range |
8015B |
Turbidity |
180.1 |
Volatile Appendix IX |
8260B |
Volatiles |
8260B |
Air Quality Laboratory
The EPD Air Quality Laboratory analyzes ambient (surrounding, breathable) air collected from monitoring stations located throughout Georgia. This laboratory also analyzes air samples collected from stationary sources (industrial or commercial facilities). Air Quality samples are collected in glass fiber filters, quartz filters, polyurethane foam plugs, carbonyl cartridges, and summa passivated canisters. They are tested for total suspended particulates, particulate matter 10 micron & 2.5 micron, lead, and other metals.. The particulates collected on the glass or quartz filters over a 24 hour period are measured to see if they exceed the 150 ug/m3 health standard. Lead and other metals are digested and analyzed by ICP/MS spectroscopy. Particles of 2.5 microns or less are given special consideration because they can enter a person’s lungs and remain there, causing potential health problems.
EPD's Air Toxics program monitors for aldehydes and ketones (such as formaldehyde and acetone), polychlorinated biphenyls (PCBs), and toxic metals (e.g., lead). EPD has established an Air Toxics Network to sample the air around Georgia.
Bacteriology Laboratory
The EPD Bacteriology Laboratory conducts analyses to find and identify bacteria in Georgia's water supplies, streams, lakes, and wastewater effluent. Microorganisms that are naturally found in our waters can have an adverse effect on human health. Coliform bacteria are a group of microorganisms that are indicators of contamination in our drinking water; fecal coliform are a direct indication of contamination from septic tanks, waste treatment plants or animal wastes.
We use multiple tube and membrane filter methods to help quantify the amount of coliform bacteria found in 100 mL of drinking water source approval and wastewater samples. A presence/absence (Colilert™) test allows EPD to routinely monitor drinking water for coliform and E. coli bacteria.
The laboratory has acquired flow cytometers and Epifluorescent microscopes. These will help in developing the methodology to identify cryptosporidium and giardia that have been found in rivers and lakes.
GC/MS (Volatiles) Laboratory
The GC/MS (Gas Chromatography Mass Spectrometer) Laboratory primarily uses GC/MS instrumentation to identify and quantify volatile compounds such as benzene, toluene, trichloroethylene, and vinyl chloride. These compounds are used in common products such as gasoline, PVC pipe, dry cleaning fluids, or paint and coating solvents. Some of these chemicals have the potential or are known human carcinogens. Semi-volatile compounds are also analyzed with GC/MS instrumentation and include compounds found in petroleum products, wood treatment and pesticide residues.
Drinking water samples collected statewide are analyzed for over 60 volatile and semi-volatile compounds, as required by federal and state environmental rules. If any compounds are detected, EPD will conduct additional sampling and investigation to determine its source. Hazardous waste samples are often analyzed for volatile and semi-volatile organics, an indication of improper disposal. Canisters of air taken from statewide ambient monitors are analyzed for photochemical oxidants (precursors to smog) and toxic organic chemicals (such as tetrachloroethylene).
Inorganics Laboratory
The Inorganic Laboratory analyzes a variety of sample types (Drinking Water, Streams and Lakes, Hazardous Waste, Water Pollution Control Plants) for over 40 different parameters. Some of the more common analytes are: Ammonia, Nitrate/Nitrite, Total Phosphorous, Nitrogen (TKN), Total Organic Carbon, Biochemical Oxygen Demand, Chemical Oxygen Demand, Turbidity, Color and Suspended Solids. These parameters give a general, overall view of Georgia's water quality. They are important in the monitoring of agricultural runoff to lakes and streams, pollution control plants, background monitoring as well as ensuring facilities are meeting their permitted discharge limits.
In addition, Nitrate/Nitrite, Sulfate, Cyanide, Phosphates and Total Organic Carbon are analyzed on Drinking Water samples throughout the state as part of the Safe Drinking Water Act. High nitrate (found in fertilizers) levels have been implicated in toxicity with infants. Sulfates and Organic Carbon can impart taste or odor to drinking water.
Metals Laboratory
The Metals Laboratory is responsible for identifying and measuring the concentration of metal ions (such as arsenic, lead, copper, mercury, or cadmium) in environmental samples. Samples of drinking water, either from water treatment plants or individual homes, are also analyzed for metals. Other water samples come from streams and lakes. Aquatic biota is thought to be especially sensitive to metals and can bio-accumulate metals in tissues. Using Inductively Coupled Plasma Spectroscopy (ICP and ICP/MS), extremely pure water and clean plastic-ware, Metals Laboratory scientists can measure metals down to a few parts per billion.
At the other extreme, the Metals Lab conducts a Toxicity Characterization Leachate Procedure (TCLP) to mimic the level of metals leached out of a sanitary landfill over many years. Above certain levels, soils contaminated with metals may need remediation or removal to ensure human health and safety.
Organics Laboratory
The Organics Lab analyzes Public Water systems for Synthetic Organic Compounds (SOCs) on a varying cycle. This comprises 12 different chemical tests and approximately 100 plus chemical compounds. These include: Pesticides (e.g., 2,4-D, chlordane) and polychlorinated biphenyls (PCBs); Trihalomethanes; and Haloacetic Acids. Trihalomethanes (e.g.,chloroform, bromodichloromethane) analyses are conducted on our larger drinking water systems. Drinking water plants add chlorine to disinfect the water before it is released for public consumption. These trihalomethane compounds are often formed from the chlorination of trace quantities of organic compounds.
The laboratory analyzes PUF (polyurethane foam) cartridges on a 12 day cycle for pesticide and polynuclear aromatic compounds. Ozone precursors like carbonyl (e.g., methyl ethyl ketone) compounds are analyzed on this same cycle plus an intensive summer sampling period.